Determination of Volatile Components of <i>Blaps rhynchoptera</i> by Headspace Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry

Jie-li SU; Bi-tao LI; Yun-song WANG; Rong-sheng LI; Xing-ping ZHANG; Long-hui BAI; Kou WANG; Zheng-qi WEN

doi:10.12259/j.issn.2095-610X.S20210802

Volume 42 Issue 8

Aug. 2021

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Article Navigation > Journal of Kunming Medical University > 2021 > 42(8): 7-10

Jie-li SU, Bi-tao LI, Yun-song WANG, Rong-sheng LI, Xing-ping ZHANG, Long-hui BAI, Kou WANG, Zheng-qi WEN. Determination of Volatile Components of Blaps rhynchoptera by Headspace Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry[J]. Journal of Kunming Medical University, 2021, 42(8): 7-10. doi: 10.12259/j.issn.2095-610X.S20210802

Citation:

Jie-li SU, Bi-tao LI, Yun-song WANG, Rong-sheng LI, Xing-ping ZHANG, Long-hui BAI, Kou WANG, Zheng-qi WEN. Determination of Volatile Components of Blaps rhynchoptera by Headspace Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry[J]. Journal of Kunming Medical University, 2021, 42(8): 7-10. doi: 10.12259/j.issn.2095-610X.S20210802

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Determination of Volatile Components of Blaps rhynchoptera by Headspace Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry

doi: 10.12259/j.issn.2095-610X.S20210802

1.
School of Pharmaceutical Science and Yunnan/Key Laboratory of Natural Pharmacology of Yunnan Province，Kunming Medical University，Kunming Yunnan 650500
2.
Dept. of Oncology，The 1st Affiliated Hospital of Kunming Medical University，Kunming Yunnan 650032
3.
Key Laboratory of Medicinal Chemistry for Natural Resource，Ministry of Education/Yunnan Research and Development Center for Natural Products/Department of Education/School of Chemical Science and Technology，Yunnan University，Kunming Yunnan 650091，China

Received Date: 2021-06-25
Available Online: 2021-08-03
Publish Date: 2021-08-04

Abstract

Abstract

Objective To determine the volatile components of the dried Blaps rhynchoptera Fairmaire. Methods Headspace solid phase microextraction （HS-SPME） combined with gas chromatography-mass spectrometry （GC-MS） were used to analysis and identify the volatile components, and the relative content of each compound was calculated using the area normalization method. Results Through mass spectrum scanning combined with mass standard library, 40 components were identified, accounting for 92.80% of the total peak area. Sixteen hydrocarbons were represented by straight-chain and branched alkanes, accounting for 35.73%. Eight fatty acids were represented by short-chain fatty acids, accounted for 35.87%. In addition, it also contained amines, alcohols, esters, aldehydes, phenols, ketones, and ethers. Tridecane, 3-methylbutyric acid, 2-methylbutyric acid, trimethylamine and acetic acid were identified as the major components, accounting for 21.47%, 16.88%, 7.67%, 6.59% and 5.47%, respectively. Conclusion Hydrocarbons and short-chain fatty acids are main volatile components in the dried B. rhynchoptera, which have a variety of pharmacological activities. The results could provide a theoretical basis for the further development and utilization of the medicinal insect resources.
- Blaps rhynchoptera Fairmaire,
- Headspace solid phase microextraction,
- Gas chromatography-Mass spectrometry,
- Volatile components

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References(18)

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