Isolation and Identification of Chemical Constituents of Ethyl Acetate Extraction Layer from Buddleja Officinalis Maxim

Fang LIU; Yun-ping GUO; Bo LIU; Chang-qi CHEN; Ya-ni GUO

doi:10.12259/j.issn.2095-610X.S20210806

Volume 42 Issue 8

Aug. 2021

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Fang LIU, Yun-ping GUO, Bo LIU, Chang-qi CHEN, Ya-ni GUO. Isolation and Identification of Chemical Constituents of Ethyl Acetate Extraction Layer from Buddleja Officinalis Maxim[J]. Journal of Kunming Medical University, 2021, 42(8): 31-34. doi: 10.12259/j.issn.2095-610X.S20210806

Citation:

Fang LIU, Yun-ping GUO, Bo LIU, Chang-qi CHEN, Ya-ni GUO. Isolation and Identification of Chemical Constituents of Ethyl Acetate Extraction Layer from Buddleja Officinalis Maxim[J]. Journal of Kunming Medical University, 2021, 42(8): 31-34. doi: 10.12259/j.issn.2095-610X.S20210806

Citation:

Fang LIU, Yun-ping GUO, Bo LIU, Chang-qi CHEN, Ya-ni GUO. Isolation and Identification of Chemical Constituents of Ethyl Acetate Extraction Layer from Buddleja Officinalis Maxim[J]. Journal of Kunming Medical University, 2021, 42(8): 31-34. doi: 10.12259/j.issn.2095-610X.S20210806

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Isolation and Identification of Chemical Constituents of Ethyl Acetate Extraction Layer from Buddleja Officinalis Maxim

doi: 10.12259/j.issn.2095-610X.S20210806

School of Pharmaceutical Science and Yunnan Key Laboratory of Pharmacology for Natural Products，Kunming Medical University，Kunming Yunnan 650500，China

Received Date: 2021-06-22
Available Online: 2021-08-03
Publish Date: 2021-08-04

Abstract

Abstract

Objective To extract and identify the chemical constituents from ethyl acetate layer of the Buddleja officinalis Maxim. Methods The chemical constituents were isolated by silica gel column chromatography, Spehadex LH-20、HPLC and other methods, and MS、¹H-NMR and ¹³C-NMR were used to identify its structure. Results 10 chemical compounds isolated and identified were α-amyrin （Ⅰ）, stigmasterol （Ⅱ）, lupeol （Ⅲ）, cycloeucalenone （Ⅳ）, ethylparaben （Ⅴ）, lupeol acetate （Ⅵ）, luteolin （Ⅶ）, ursolic acid （Ⅷ）, α-spinasterol （Ⅸ）, linarin （Ⅹ）. Conclusion Ⅰ, Ⅱ, Ⅲ, Ⅴ, Ⅷ are the first isolates from the Buddleja officinalis.
- Buddleja officinalis Maxim,
- Chemical constituents,
- Structure identification

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References(12)

References

[1]	郭雷,朱文成,刘超. 密蒙花化学成分及生物活性研究进展[J]. 食品研究与开发,2012,33(7):222-225. doi: 10.3969/j.issn.1005-6521.2012.07.063
[2]	杨东方,胡云飞,丁倩倩,等. 密蒙花的化学成分及质量控制方法研究进展[J]. 中国现代应用药学,2019,36(22):2870-2875.
[3]	Yan Huang,Xu Wu,Jianwen Wen,et al. A Study on the Chemical Constituents of Pileasinofasciata C. J. Chen[J]. Medicinal Plant,2017,8(3):1-4.
[4]	薛鹏辉,段静诗,丁丽琴,等. 鹅不食草中甾体及酚类化学成分研究[J]. 中国药物化学杂志,2020,30(6):340-346.
[5]	孙志青,刘立云,孙岩,等. 血芙蓉化学成分的研究[J]. 中成药,2020,42(4):932-938. doi: 10.3969/j.issn.1001-1528.2020.04.021
[6]	吴贵辉,陈艳,郑黎花,等. 黔产杜仲化学成分研究[J]. 中药材,2015,38(5):980-984.
[7]	张鹏耀,舒任庚,严喜鸾,等. 山蜡梅化学成分研究[J]. 中国药学杂志,2017,52(18):1594-1596.
[8]	Chen Hui,Li Yu Jie,Sun Yan Jun,et al. Antihyperlipidemic glycosides from the root bark of Lyciumchinense.[J]. Natural Product Research,2019,33(18):2655-2661. doi: 10.1080/14786419.2018.1466125
[9]	何丽丽,姚彩云,闫炳雄,等. 壮药山风中的黄酮类化学成分研究[J]. 中国现代中药,2019,21(8):1016-1020.
[10]	孙彦君,陈豪杰,高美玲,等. 小驳骨中萜类化学成分研究[J]. 中草药,2020,51(2):293-298.
[11]	刘宝,胡飞龙,雷福厚,等. 灰色紫金牛化学成分研究[J]. 中药材,2019,42(3):560-562.
[12]	郑畅,阮静雅,瞿璐,等. 密蒙花中黄酮类成分的分离与鉴定[J]. 中国药物化学杂志,2018,28(1):52-57.

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