Isolation and Identification of Chemical Constituents of Ethyl Acetate Extraction Layer from Buddleja Officinalis Maxim

Fang LIU; Yun-ping GUO; Bo LIU; Chang-qi CHEN; Ya-ni GUO

doi:10.12259/j.issn.2095-610X.S20210806

Volume 42 Issue 8

Aug. 2021

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Fang LIU, Yun-ping GUO, Bo LIU, Chang-qi CHEN, Ya-ni GUO. Isolation and Identification of Chemical Constituents of Ethyl Acetate Extraction Layer from Buddleja Officinalis Maxim[J]. Journal of Kunming Medical University, 2021, 42(8): 31-34. doi: 10.12259/j.issn.2095-610X.S20210806

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Isolation and Identification of Chemical Constituents of Ethyl Acetate Extraction Layer from Buddleja Officinalis Maxim

doi: 10.12259/j.issn.2095-610X.S20210806

School of Pharmaceutical Science and Yunnan Key Laboratory of Pharmacology for Natural Products，Kunming Medical University，Kunming Yunnan 650500，China

Received Date: 2021-06-22
Available Online: 2021-08-03
Publish Date: 2021-08-04

Abstract

Abstract

Objective To extract and identify the chemical constituents from ethyl acetate layer of the Buddleja officinalis Maxim. Methods The chemical constituents were isolated by silica gel column chromatography, Spehadex LH-20、HPLC and other methods, and MS、¹H-NMR and ¹³C-NMR were used to identify its structure. Results 10 chemical compounds isolated and identified were α-amyrin （Ⅰ）, stigmasterol （Ⅱ）, lupeol （Ⅲ）, cycloeucalenone （Ⅳ）, ethylparaben （Ⅴ）, lupeol acetate （Ⅵ）, luteolin （Ⅶ）, ursolic acid （Ⅷ）, α-spinasterol （Ⅸ）, linarin （Ⅹ）. Conclusion Ⅰ, Ⅱ, Ⅲ, Ⅴ, Ⅷ are the first isolates from the Buddleja officinalis.
- Buddleja officinalis Maxim,
- Chemical constituents,
- Structure identification

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References

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